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Cross-Polarization Dynamics in Polycrystalline Samples
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https://doi.org/10.1016/j.molstruc.2006.07.06Abstract
We observe non-monotonic development of the 13C magnetization in polycrystalline samples of glycine, sucrose, and adamantine during cross-polarization. We demonstrate, by fitting the time dependence, that the development quantitatively results from dipolar oscillations. To fit the data quantitatively requires one to assume two types of spin-diffusion behavior.
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