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Synthesis, characterization and properties of a glycol-coordinated ε-Keggin-type Al 13 chloride
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https://doi.org/10.1039/c8cc01363bAbstract
Herein we present the first example of a glycol-coordinated ε-Keggin Al13 chloride (gl-ε-Al13), which is the first chelated version since discovery of Al13 in 1960. The molecular structure consists of [AlO4Al12(OH)12(OC2H4OH)12]Cl7·H2O units with chelating mono-anionic ethylene glycol units replacing one bridging and one terminal oxygen site.
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