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Crystallization and preliminary X-ray analysis of the vitamin D-binding protein from human serum
Abstract
The vitamin D-binding protein from human serum has been crystallized from polyethylene glycol as a complex with 25-hydroxyvitamin D3 and examined by X-ray diffraction photography. The space group of the crystals is C2 with a = 203.0 A ̊, b = 75.8 A ̊, c = 90.9 A ̊ and β = 109.5°. There are two molecules of 56,000 dalton in the asymmetric unit. The crystals diffract to about 3.0 Å resolution but the patterns exhibit a substantial level of diffuse scatter. © 1985.
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