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Synthesis of 9-borafluorene analogues featuring a three-dimensional 1,1′-bis( o -carborane) backbone
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https://doi.org/10.1039/c8cc10087jAbstract
The synthesis of [1,1'-bis(o-carboranyl)]boranes was achieved through the deprotonation of 1,1'-bis(o-carborane) reagents followed by salt metathesis with (iPr)2NBCl2. X-ray crystallography confirms planar central BC4 rings and Gutmann-Beckett studies reveal an increase in Lewis acidity at the boron center in comparison to their biphenyl congener, 9-borafluorene.
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