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Hydrothermal synthesis and characterization of mixed-valence hexatungstates: crystal structures of [(C2H5)(4)N](3)[(WW5O19)-W-V-O-VI]center dot 0.5H(2)O and [H3N(CH2)(2)NH3](2)[(WW5O19)-W-V-O-VI]center dot[H2N(CH2)(2)NH2]Cl center dot 8H(2)O

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